This is summarizes the synthesis characterization and photocatalytic activity of carbonaceous and TiO2 nanocomposite for efficient hydrogen production. In this developed various catalysts such as TiO2 doped AC FCNT-TiO2 TiO2 decorated on MWCNTs graphitic-carbon-TiO2 Cu/FCNT-TiO2 QDs ternary catalysts through hydrothermal solvothermal and wet impregnation process. The mentioned catalysts crystallinity morphology recombination rate light absorption strength composition elements and surface area results investigated by the X-ray diffraction Transmission Electron Microscopy Photoluminescence spectra Ultraviolet-visible Diffused Reflectance Spectra X-ray Photoelectron Spectroscopy and Fourier Transform Infra-Red Spectroscopy advanced characterization techniques. The synthesized catalysts hydrogen production evolved under natural solar-light and some catalyst activities under solar simulator. Furthermore the hydrogen test also done by using seawater with AC-TiO2 catalyst. The hydrogen production was analysed with Gas Chromatograph (Shimadzu GC-2014) equipped thermal conductivity detector (TCD) and molecular sieves/5A° column under a constant flow of nitrogen gas.
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